Appendix 2 Lab Sample Container, Preservation, and Hold Times for Sediments and Tissues

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TYPE OF ANALYSIS SIZE TYPE PRESERVATION HOLD TIME

SEDIMENTS, TISSUES AND ORGANICS

General chemistry 200 g P, W keep cool, 4°C 72 h

EOX, Extractable Organic Halides 50 g G, Solv, Fc freeze (dry ice) 6 mo

Metals 100 g P, W (T) keep cool, 4°C 72 h

Organic Carbon 100 g P or G keep cool, 4°C 72 h

Organics - Semivolatile 200 g G, A, W, Solv freeze (dry ice) 6 mo

Organics - Volatile 50 g G, W, Solv, B freeze (dry ice) 14 d

Particle Size Analysis 100 g dry wt P or G keep cool, 4°C 72 h

PQ-8 (copper 8, copper quinolate) 100 g G (A), W, Solv freeze (dry ice) 6 mo

ANALYSES WITH LIMITED SHELF LIFE

pH, Turbidity, Acidity, Alkalinity 72 h

Ammonia, TKN, Nitrate, Nitrite 72 h

Portho, total, total dissolved 72 h

bacteria 48 h

LEGEND

P = plastic G = glass

B = Baked T = Tissue Cup

Solv = solvent cleaned A = amber

Fc = foil lined cap W = wide mouth


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